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DARIN, Gaspar, Kengo IMAKUMA, Rafael Trautwein SANTIAGO, Klebson Lucenildo DA SILVA, Luiz Fernardo CÓTICA, Martin FABIÁN, Jan VALÍČEK, Horst HAHN and Vladimír ŠEPEĽÁK. X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes. Data in Brief. Netherlands: Elsevier BV, 2021, volume 35, April 2021, p. 106972-106977. ISSN 2352-3409.
Other formats: BibTeX LaTeX RIS @article{58801, author = {Darin, Gaspar and Imakuma, Kengo and Santiago, Rafael Trautwein and Da Silva, Klebson Lucenildo and Cótica, Luiz Fernardo and Fabián, Martin and Valíček, Jan and Hahn, Horst and Šepeľák, Vladimír}, article_location = {Netherlands}, article_number = {April 2021}, keywords = {Gd6UO12; Rietveld refinement; XRD; Thermal analysis; Mechanochemistry}, language = {eng}, issn = {2352-3409}, journal = {Data in Brief}, title = {X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes}, url = {https://www.sciencedirect.com/science/article/pii/S2352340921002560?via%3Dihub}, volume = {volume 35}, year = {2021} } TY - JOUR ID - 58801 AU - Darin, Gaspar - Imakuma, Kengo - Santiago, Rafael Trautwein - Da Silva, Klebson Lucenildo - Cótica, Luiz Fernardo - Fabián, Martin - Valíček, Jan - Hahn, Horst - Šepeľák, Vladimír PY - 2021 TI - X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes JF - Data in Brief VL - volume 35 IS - April 2021 SP - 106972-106977 EP - 106972-106977 PB - Elsevier BV SN - 23523409 KW - Gd6UO12 KW - Rietveld refinement KW - XRD KW - Thermal analysis KW - Mechanochemistry UR - https://www.sciencedirect.com/science/article/pii/S2352340921002560?via%3Dihub N2 - The datasets presented here are related to the research paper entitled “Disordered Gd6UO12-δ with the cation antisite defects prepared by a combined mechanochemical−thermal method” [1]. The datasets complement the findings [1] on the effect of the combined mechanochemical−thermal processing of the stoichiometric mixture of solid pre cursors (3Gd2O3 + UO2) on the formation of Gd6UO12-δ phase. In this article, we provide (i) X-ray diffraction (XRD) data of the 3Gd2O3 + UO2 mixture milled for 12 h, (ii) the refined XRD data of the non-milled 3Gd2O3 + UO2 mixture after annealing at 1282 °C for 3 h in air, and (iii) the thermogravimetric and differential thermal analysis (TG-DTA) data for non-milled and mechanically preactivated3Gd2O3+UO2 mixturemeasuredinairataheatrateof 10K/min. ER - DARIN, Gaspar, Kengo IMAKUMA, Rafael Trautwein SANTIAGO, Klebson Lucenildo DA SILVA, Luiz Fernardo CÓTICA, Martin FABIÁN, Jan VALÍČEK, Horst HAHN and Vladimír ŠEPEĽÁK. X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes. \textit{Data in Brief}. Netherlands: Elsevier BV, 2021, volume 35, April 2021, p.~106972-106977. ISSN~2352-3409.

DARIN, Gaspar, Kengo IMAKUMA, Rafael Trautwein SANTIAGO, Klebson Lucenildo DA SILVA, Luiz Fernardo CÓTICA, Martin FABIÁN, Jan VALÍČEK, Horst HAHN and Vladimír ŠEPEĽÁK. X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes. Data in Brief. Netherlands: Elsevier BV, 2021, volume 35, April 2021, p. 106972-106977. ISSN 2352-3409.

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Basic information
Original name	X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes
Authors	DARIN, Gaspar (guarantor), Kengo IMAKUMA, Rafael Trautwein SANTIAGO, Klebson Lucenildo DA SILVA, Luiz Fernardo CÓTICA, Martin FABIÁN, Jan VALÍČEK (203 Czech Republic, belonging to the institution), Horst HAHN and Vladimír ŠEPEĽÁK (703 Slovakia, belonging to the institution).
Edition	Data in Brief, Netherlands, Elsevier BV, 2021, 2352-3409.

Other information
Original language	English
Type of outcome	Article in a journal
Field of Study	20501 Materials engineering
Country of publisher	Netherlands
Confidentiality degree	is not subject to a state or trade secret
WWW	URL
Organization unit	Institute of Technology and Business in České Budějovice
Keywords in English	Gd6UO12; Rietveld refinement; XRD; Thermal analysis; Mechanochemistry
Tags	KSTR5, RIV21, SCOPUS
Changed by	Changed by: Mgr. Nikola Vyhlidalová, učo 28324. Changed: 25/6/2021 07:56.

Abstract
The datasets presented here are related to the research paper entitled “Disordered Gd6UO12-δ with the cation antisite defects prepared by a combined mechanochemical−thermal method” [1]. The datasets complement the findings [1] on the effect of the combined mechanochemical−thermal processing of the stoichiometric mixture of solid pre cursors (3Gd2O3 + UO2) on the formation of Gd6UO12-δ phase. In this article, we provide (i) X-ray diffraction (XRD) data of the 3Gd2O3 + UO2 mixture milled for 12 h, (ii) the refined XRD data of the non-milled 3Gd2O3 + UO2 mixture after annealing at 1282 °C for 3 h in air, and (iii) the thermogravimetric and differential thermal analysis (TG-DTA) data for non-milled and mechanically preactivated3Gd2O3+UO2 mixturemeasuredinairataheatrateof 10K/min.

Abstract

The datasets presented here are related to the research paper entitled “Disordered Gd6UO12-δ with the cation antisite defects prepared by a combined mechanochemical−thermal method” [1]. The datasets complement the findings [1] on the effect of the combined mechanochemical−thermal processing of the stoichiometric mixture of solid pre cursors (3Gd2O3 + UO2) on the formation of Gd6UO12-δ phase. In this article, we provide (i) X-ray diffraction (XRD) data of the 3Gd2O3 + UO2 mixture milled for 12 h, (ii) the refined XRD data of the non-milled 3Gd2O3 + UO2 mixture after annealing at 1282 °C for 3 h in air, and (iii) the thermogravimetric and differential thermal analysis (TG-DTA) data for non-milled and mechanically preactivated3Gd2O3+UO2 mixturemeasuredinairataheatrateof 10K/min.