DARIN, Gaspar, Kengo IMAKUMA, Rafael Trautwein SANTIAGO, Klebson Lucenildo DA SILVA, Luiz Fernardo CÓTICA, Martin FABIÁN, Jan VALÍČEK, Horst HAHN a Vladimír ŠEPEĽÁK. X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes. Data in Brief. Netherlands: Elsevier BV, 2021, volume 35, April 2021, s. 106972-106977. ISSN 2352-3409. |
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@article{58801, author = {Darin, Gaspar and Imakuma, Kengo and Santiago, Rafael Trautwein and Da Silva, Klebson Lucenildo and Cótica, Luiz Fernardo and Fabián, Martin and Valíček, Jan and Hahn, Horst and Šepeľák, Vladimír}, article_location = {Netherlands}, article_number = {April 2021}, keywords = {Gd6UO12; Rietveld refinement; XRD; Thermal analysis; Mechanochemistry}, language = {eng}, issn = {2352-3409}, journal = {Data in Brief}, title = {X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes}, url = {https://www.sciencedirect.com/science/article/pii/S2352340921002560?via%3Dihub}, volume = {volume 35}, year = {2021} }
TY - JOUR ID - 58801 AU - Darin, Gaspar - Imakuma, Kengo - Santiago, Rafael Trautwein - Da Silva, Klebson Lucenildo - Cótica, Luiz Fernardo - Fabián, Martin - Valíček, Jan - Hahn, Horst - Šepeľák, Vladimír PY - 2021 TI - X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes JF - Data in Brief VL - volume 35 IS - April 2021 SP - 106972-106977 EP - 106972-106977 PB - Elsevier BV SN - 23523409 KW - Gd6UO12 KW - Rietveld refinement KW - XRD KW - Thermal analysis KW - Mechanochemistry UR - https://www.sciencedirect.com/science/article/pii/S2352340921002560?via%3Dihub N2 - The datasets presented here are related to the research paper entitled “Disordered Gd6UO12-δ with the cation antisite defects prepared by a combined mechanochemical−thermal method” [1]. The datasets complement the findings [1] on the effect of the combined mechanochemical−thermal processing of the stoichiometric mixture of solid pre cursors (3Gd2O3 + UO2) on the formation of Gd6UO12-δ phase. In this article, we provide (i) X-ray diffraction (XRD) data of the 3Gd2O3 + UO2 mixture milled for 12 h, (ii) the refined XRD data of the non-milled 3Gd2O3 + UO2 mixture after annealing at 1282 °C for 3 h in air, and (iii) the thermogravimetric and differential thermal analysis (TG-DTA) data for non-milled and mechanically preactivated3Gd2O3+UO2 mixturemeasuredinairataheatrateof 10K/min. ER -
DARIN, Gaspar, Kengo IMAKUMA, Rafael Trautwein SANTIAGO, Klebson Lucenildo DA SILVA, Luiz Fernardo CÓTICA, Martin FABIÁN, Jan VALÍČEK, Horst HAHN a Vladimír ŠEPEĽÁK. X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes. \textit{Data in Brief}. Netherlands: Elsevier BV, 2021, volume 35, April 2021, s.~106972-106977. ISSN~2352-3409.
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