X-ray diffraction and thermoanalytical datasets of precursors
of the Gd6UO12-δ phase processed by combined
mechanochemical−thermal routes

J 2021

X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes

DARIN, Gaspar; Kengo IMAKUMA; Rafael Trautwein SANTIAGO; Klebson Lucenildo DA SILVA; Luiz Fernardo CÓTICA et. al.

Basic information

Original name

X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes

Authors

DARIN, Gaspar (guarantor); Kengo IMAKUMA; Rafael Trautwein SANTIAGO; Klebson Lucenildo DA SILVA; Luiz Fernardo CÓTICA; Martin FABIÁN; Jan VALÍČEK (203 Czech Republic, belonging to the institution); Horst HAHN and Vladimír ŠEPEĽÁK (703 Slovakia, belonging to the institution)

Edition

Data in Brief, Netherlands, Elsevier BV, 2021, 2352-3409

Other information

Language

English

Type of outcome

Article in a journal

Field of Study

20501 Materials engineering

Country of publisher

Netherlands

Confidentiality degree

is not subject to a state or trade secret

References:

URL

RIV identification code

RIV/75081431:_____/21:00002095

Organization unit

Institute of Technology and Business in České Budějovice

EID Scopus

2-s2.0-85103138509

Keywords in English

Gd6UO12; Rietveld refinement; XRD; Thermal analysis; Mechanochemistry

Abstract

V originále

The datasets presented here are related to the research paper entitled “Disordered Gd6UO12-δ with the cation antisite defects prepared by a combined mechanochemical−thermal method” [1]. The datasets complement the findings [1] on the effect of the combined mechanochemical−thermal processing of the stoichiometric mixture of solid pre cursors (3Gd2O3 + UO2) on the formation of Gd6UO12-δ phase. In this article, we provide (i) X-ray diffraction (XRD) data of the 3Gd2O3 + UO2 mixture milled for 12 h, (ii) the refined XRD data of the non-milled 3Gd2O3 + UO2 mixture after annealing at 1282 °C for 3 h in air, and (iii) the thermogravimetric and differential thermal analysis (TG-DTA) data for non-milled and mechanically preactivated3Gd2O3+UO2 mixturemeasuredinairataheatrateof 10K/min.

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Cite

DARIN, Gaspar; Kengo IMAKUMA; Rafael Trautwein SANTIAGO; Klebson Lucenildo DA SILVA; Luiz Fernardo CÓTICA; Martin FABIÁN; Jan VALÍČEK; Horst HAHN and Vladimír ŠEPEĽÁK. X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes. Data in Brief. Netherlands: Elsevier BV, 2021, volume 35, April 2021, p. 106972-106977. ISSN 2352-3409.

@article{58801,
   author = {Darin, Gaspar and Imakuma, Kengo and Santiago, Rafael Trautwein and Da Silva, Klebson Lucenildo and Cótica, Luiz Fernardo and Fabián, Martin and Valíček, Jan and Hahn, Horst and Šepeľák, Vladimír},
   article_location = {Netherlands},
   article_number = {April 2021},
   keywords = {Gd6UO12; Rietveld refinement; XRD; Thermal analysis; Mechanochemistry},
   language = {eng},
   issn = {2352-3409},
   journal = {Data in Brief},
   title = {X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes},
   url = {https://www.sciencedirect.com/science/article/pii/S2352340921002560?via%3Dihub},
   volume = {volume 35},
   year = {2021}
}

TY  - JOUR
ID  - 58801
AU  - Darin, Gaspar - Imakuma, Kengo - Santiago, Rafael Trautwein - Da Silva, Klebson Lucenildo - Cótica, Luiz Fernardo - Fabián, Martin - Valíček, Jan - Hahn, Horst - Šepeľák, Vladimír
PY  - 2021
TI  - X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes
JF  - Data in Brief
VL  - volume 35
IS  - April 2021
SP  - 106972-106977
EP  - 106972-106977
PB  - Elsevier BV
SN  - 23523409
KW  - Gd6UO12
KW  - Rietveld refinement
KW  - XRD
KW  - Thermal analysis
KW  - Mechanochemistry
UR  - https://www.sciencedirect.com/science/article/pii/S2352340921002560?via%3Dihub
N2  - The datasets presented here are related to the research paper entitled “Disordered Gd6UO12-δ with the cation antisite defects prepared by a combined mechanochemical−thermal method” [1]. The datasets complement the findings [1] on the effect of the combined mechanochemical−thermal processing of the stoichiometric mixture of solid pre cursors (3Gd2O3 + UO2) on the formation of Gd6UO12-δ phase. In this article, we provide (i) X-ray diffraction (XRD) data of the 3Gd2O3 + UO2 mixture milled for 12 h, (ii) the refined XRD data of the non-milled 3Gd2O3 + UO2 mixture after annealing at 1282 °C for 3 h in air, and (iii) the thermogravimetric and differential thermal analysis (TG-DTA) data for non-milled and mechanically preactivated3Gd2O3+UO2 mixturemeasuredinairataheatrateof 10K/min.
ER  -

DARIN, Gaspar; Kengo IMAKUMA; Rafael Trautwein SANTIAGO; Klebson Lucenildo DA SILVA; Luiz Fernardo CÓTICA; Martin FABIÁN; Jan VALÍČEK; Horst HAHN and Vladimír ŠEPEĽÁK. X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes. \textit{Data in Brief}. Netherlands: Elsevier BV, 2021, volume 35, April 2021, p.~106972-106977. ISSN~2352-3409.

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