DARIN, Gaspar, Kengo IMAKUMA, Rafael Trautwein SANTIAGO, Klebson Lucenildo DA SILVA, Luiz Fernardo CÓTICA, Martin FABIÁN, Jan VALÍČEK, Horst HAHN and Vladimír ŠEPEĽÁK. X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes. Data in Brief. Netherlands: Elsevier BV, 2021, volume 35, April 2021, p. 106972-106977. ISSN 2352-3409.
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Basic information
Original name X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes
Authors DARIN, Gaspar (guarantor), Kengo IMAKUMA, Rafael Trautwein SANTIAGO, Klebson Lucenildo DA SILVA, Luiz Fernardo CÓTICA, Martin FABIÁN, Jan VALÍČEK (203 Czech Republic, belonging to the institution), Horst HAHN and Vladimír ŠEPEĽÁK (703 Slovakia, belonging to the institution).
Edition Data in Brief, Netherlands, Elsevier BV, 2021, 2352-3409.
Other information
Original language English
Type of outcome Article in a journal
Field of Study 20501 Materials engineering
Country of publisher Netherlands
Confidentiality degree is not subject to a state or trade secret
WWW URL
Organization unit Institute of Technology and Business in České Budějovice
Keywords in English Gd6UO12; Rietveld refinement; XRD; Thermal analysis; Mechanochemistry
Tags KSTR5, RIV21, SCOPUS
Changed by Changed by: Mgr. Nikola Vyhlidalová, učo 28324. Changed: 25/6/2021 07:56.
Abstract
The datasets presented here are related to the research paper entitled “Disordered Gd6UO12-δ with the cation antisite defects prepared by a combined mechanochemical−thermal method” [1]. The datasets complement the findings [1] on the effect of the combined mechanochemical−thermal processing of the stoichiometric mixture of solid pre cursors (3Gd2O3 + UO2) on the formation of Gd6UO12-δ phase. In this article, we provide (i) X-ray diffraction (XRD) data of the 3Gd2O3 + UO2 mixture milled for 12 h, (ii) the refined XRD data of the non-milled 3Gd2O3 + UO2 mixture after annealing at 1282 °C for 3 h in air, and (iii) the thermogravimetric and differential thermal analysis (TG-DTA) data for non-milled and mechanically preactivated3Gd2O3+UO2 mixturemeasuredinairataheatrateof 10K/min.
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